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Notes for exam in jan

Quiz yourself by thinking what should be in each of the black spaces below before clicking on it to display the answer.
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Question
Answer
What is the mobile Phase in TLC?   Solvent (Normally alcohol)  
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What is the mobile Phase in Gas Chromatography?   Inert Gas (Helium)  
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How does separation occur in Chromatography?   Solid mobile phase - Adsorption Liquid mobile phase - Solubility  
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What is Retention factor?   (Distance moved by Component)/(distance moved by solvent front)  
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Why is TMS used in NMR?   1 Environment - one peak Many protons - sharp peak  
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How do you remove the OH peak from an NMR spectrum?   Add Deuterium, and shake, then repeat.  
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Oxidation of propane-1-ol will form what?   propanal (distillation) Propanoic acid (reflux)  
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oxidation of propane-2-ol will form what?   propanone (reflux)  
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reduction of butanoic acid will form?   butanol  
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The joining of ethanol and octanoic acid, with a small molecule of water removed, is?   esterification - it will form ethyl octanoate.  
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Carbonyl compounds produce what, when added to 2,4 - DNPH?   Orange Precipitate  
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What are the reagents for nitration of benzene?   HNO3 and H2SO4 conditions: 50 degrees celcius  
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What are the reagents for diazotisation?   NaNO2 and HCl (HONO) Below 10 degrees celcius  
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How do you turn diazonium chloride into an azodye?   add phenol and NaOH, the Na removes the Cl, and the Phenol adds to the salt.  
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What is the most reactive halogen?   fluorine  
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