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Gen Chem (1)

QuestionAnswer
What is a beaker used for? Heating, mixing, or stirring solutions. Wide-mouth with a spout. NOT accurate for measuring volumes.
What is a graduated cylinder used for? Measuring liquid volumes. Narrower and taller than beakers. More accurate than beakers, but pipettes/burettes/volumetric flasks are better for high accuracy.
What are test tubes used for? Holding small volumes, mixing, comparing samples by color. Can be heated, cooled, or stored. NOT used to measure volumes.
What is an Erlenmeyer flask used for? Mixing, heating, stirring, and swirling solutions. Preferred over beakers for swirling (less spill risk). Also used in titrations. NOT accurate for volume measurement.
What is a volumetric flask used for? Obtaining a very specific volume of liquid (single marking on neck). Used for preparing or diluting solutions. Capped to prevent evaporation.
What is a boiling flask (round-bottom flask) used for? Swirling and heating liquids. Requires a clamp or corkscrew ring to stand. NOT used to measure volumes.
What are droppers (Pasteur pipettes) used for? Delivering liquid (usually an indicator) in a drop-wise fashion. Small glass tube with a rubber bulb.
What are pipettes used for? The most precise glassware for measuring and transferring a specific volume of liquid. Can be graduated, volumetric, or electronic.
What is a burette used for? Dispensing highly precise volumes of liquid. Used in titrations to deliver a titrant. Has a stopcock to control flow. Long, graduated glass tube.
What is a Bunsen burner used for? Producing an open flame for heating. Connected to natural gas via rubber tubing. Has a valve (gas flow) and collar (airflow). Lit with a striker.
What is a pH meter used for? Accurately measuring the pH of a solution. Must be calibrated before each use.
What is a digital balance used for? Accurately measuring the mass of a solid sample. The "tare" button resets the reading to zero to exclude the weight of the container.
What is a meniscus and how do you read it? The curved surface of a liquid in glassware — higher at the edges, lower at the center. Always read from the bottom of the meniscus with eyes level to the glassware.
How do you calculate volume in a reverse-numbered burette? Volume = V(total) − V(reading). Example: if the burette reads 11 mL and total volume is 50 mL, then volume = 50 − 11 = 39 mL.
What is the order of precision for volume measurement (most to least)? Pipettes > Burettes/Volumetric Flasks > Graduated Cylinders > Beakers/Erlenmeyer Flasks.
What does "volumetric" glassware mean vs. "graduated"? Volumetric = single marking for one specific volume (more precise). Graduated = multiple markings for different volumes (less precise).
How do you properly measure the mass of a solid sample? Place weighing paper or glassware on the balance first, press tare to zero it out, then add the sample. Never place the sample directly on the balance.
What is centrifugation? A process using a centrifuge to separate mixture components by spinning at high speeds. Denser solids form a pellet at the bottom; liquid supernatant sits on top.
How do you separate a solid pellet from liquid supernatant after centrifugation? Use a pipette to remove the liquid, or decant (pour off) the liquid, leaving the solid behind. Filtration can also be used.
What is titration? A method of delivering a titrant drop-by-drop via a burette to a solution to determine the unknown concentration. The equivalence point is when the titrant has completely reacted with the reagent.
What is the difference between equivalence point and endpoint in titration? Equivalence point = titrant has completely reacted with the reagent. Endpoint = observable change (e.g., color change). Any deviation between them is titration error.
What is calorimetry? A method to measure heat energy released or absorbed during a chemical reaction. Basic setup uses a Styrofoam cup, lid, and thermometer. Determines if a reaction is exothermic (releases heat) or endothermic (absorbs heat).
What is a safety shower used for? Delivers a continuous stream of water for anyone splashed with toxic/corrosive chemicals or whose clothing has caught fire.
What is an eye wash station used for? Treats chemical splashes in or near the eyes. Rinse thoroughly with both eyes open.
What is a fume hood used for? Provides ventilation to minimize exposure to harmful vapors. Volatile substance containers should be covered with a watch glass when not in use.
When should fire extinguishers be used and how? For solvent or electrical fires only (NOT paper or wood). Aim at the base of the fire closest to you. Position yourself between the fire and the exit.
What personal protective equipment (PPE) is required in the lab? Lab coat, safety goggles, gloves, and closed-toed shoes. Avoid contact lenses even with goggles — fumes can concentrate underneath.
How should broken glass be handled? Clean up immediately and carefully using a dustpan. Dispose of in the designated broken glass container.
How do you properly dispose of chemical solutions? Acids, alkalis, and water-miscible solutions can be poured down the drain with water. Organic and water-immiscible chemicals go in the appropriate waste bin — NOT down the drain.
What are three things you should NEVER do in the lab? Never eat or drink in the lab, never add water directly to concentrated acid (add acid to water instead), and never pipette by mouth.
What is accuracy vs. precision? Accuracy = how close a measurement is to the true/literature value. Precision = how consistent repeated measurements are with each other. A value can be precise but inaccurate, or accurate but imprecise.
What are the four rules for significant digits? 1) All non-zero digits are significant. 2) Zeros between two non-zero digits are significant. 3) Trailing zeros after a decimal point are significant. 4) All other zeros are NOT significant (e.g., 500 or 0.003).
How do you handle significant digits in multiplication/division? Round the answer to the same number of sig figs as the measurement with the fewest sig figs.
How do you handle significant digits in addition/subtraction? Round the answer to the least precise decimal place among all measurements.
What is systematic error? Error consistently skewed in one direction by the same amount each time. Caused by faulty equipment or procedural errors (e.g., forgetting to tare the balance).
What is random error? Error that varies in direction and magnitude each time. Caused by human error (e.g., inconsistent meniscus readings, reaction time with a stopwatch).
What is the formula for percent error? % error = (|experimental − actual| / actual) × 100%
What is decanting? A separation technique where the liquid (supernatant) is simply poured out of a vessel, leaving the solid behind. Commonly used after centrifugation to separate the liquid supernatant from the solid pellet.
Created by: smurtab
 

 



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